Scientific American Supplement, No. 514, November 7, 1885 by Various
page 53 of 133 (39%)
page 53 of 133 (39%)
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SANDMANN'S VINEGAR APPARATUS.
For obtaining anhydrous or very concentrated vinegar directly from pyrolignite of lime or other acetates by a single distillation, Mr. D. Sandmann, of Charlottenburg, employs the apparatus shown in the accompanying engraving. It consists of a double-bottomed copper or enameled iron boiler, A, arranged for being heated by steam, and the upper part of which is protected against the action of the acid vapors disengaged during distillation by a lining of refractory clay. The stone cover, B, is provided with an aperture, b, through which the boiler is filled. The steam pipe, k, is inclosed in a second pipe, f, provided with radii. This tube serves as a stirrer; and is set in motion by means of a pulley, g. The tube, c, is connected with a worm, h, and the tube, d, which is provided with a valve, leads to the second boiler, C. The head, D, which acts, by reason of its internal arrangement, as a dephlegmator, is of enameled iron, and is provided with a thermometer, f, and an aperture, p. Above the spirals of the worm, e, are placed strips of glass, the free intervals between which are filled in with pieces of glass, porcelain, or any other material not attackable by acids. The arrangement is such that the rising vapors can regularly and without obstruction traverse these materials of wide surface. The condensed liquid falls back into the lower part of the boiler. The worm, e, debouches into a cooler, F, fed with water through the cock, n. At the bottom of the boiler, A, there is fixed a tubulure, r, closed by a lever, s, and having a fastening device, o. This tubulure permits of emptying the boiler into the reservoir, L. A like arrangement is found in the boiler, C. The valves, V, serve to |
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