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An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 16 of 272 (05%)
time in subsequent filtrations or evaporations.

All stirring rods employed in quantitative analyses should be rounded
at the ends by holding them in the flame of a burner until they begin
to soften. If this is not done, the rods will scratch the inner
surface of beakers, causing them to crack on subsequent heating.


EVAPORATION OF LIQUIDS

The greatest care must be taken to prevent loss of solutions during
processes of evaporation, either from too violent ebullition, from
evaporation to dryness and spattering, or from the evolution of gas
during the heating. In general, evaporation upon the steam bath is to
be preferred to other methods on account of the impossibility of
loss by spattering. If the steam baths are well protected from dust,
solutions should be left without covers during evaporation; but
solutions which are boiled upon the hot plate, or from which gases are
escaping, should invariably be covered. In any case a watch-glass may
be supported above the vessel by means of a glass triangle, or other
similar device, and the danger of loss of material or contamination by
dust thus be avoided. It is obvious that evaporation is promoted by
the use of vessels which admit of the exposure of a broad surface to
the air.

Liquids which contain suspended matter (precipitates) should always
be cautiously heated, since the presence of the solid matter is
frequently the occasion of violent "bumping," with consequent risk to
apparatus and analysis.

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