An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 16 of 272 (05%)
page 16 of 272 (05%)
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time in subsequent filtrations or evaporations.
All stirring rods employed in quantitative analyses should be rounded at the ends by holding them in the flame of a burner until they begin to soften. If this is not done, the rods will scratch the inner surface of beakers, causing them to crack on subsequent heating. EVAPORATION OF LIQUIDS The greatest care must be taken to prevent loss of solutions during processes of evaporation, either from too violent ebullition, from evaporation to dryness and spattering, or from the evolution of gas during the heating. In general, evaporation upon the steam bath is to be preferred to other methods on account of the impossibility of loss by spattering. If the steam baths are well protected from dust, solutions should be left without covers during evaporation; but solutions which are boiled upon the hot plate, or from which gases are escaping, should invariably be covered. In any case a watch-glass may be supported above the vessel by means of a glass triangle, or other similar device, and the danger of loss of material or contamination by dust thus be avoided. It is obvious that evaporation is promoted by the use of vessels which admit of the exposure of a broad surface to the air. Liquids which contain suspended matter (precipitates) should always be cautiously heated, since the presence of the solid matter is frequently the occasion of violent "bumping," with consequent risk to apparatus and analysis. |
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