An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 22 of 272 (08%)
page 22 of 272 (08%)
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and lowering the beams works smoothly; (3) that the pan-arrests touch
the pans when the beam is lowered; and (4) that the needle swings equal distances on either side of the zero-point when set in motion without any load on the pans. If the latter condition is not fulfilled, the balance should be adjusted by means of the adjusting screw at the end of the beam unless the variation is not more than one division on the scale; it is often better to make a proper allowance for this small zero error than to disturb the balance by an attempt at correction. Unless a student thoroughly understands the construction of a balance he should never attempt to make adjustments, but should apply to the instructor in charge. The object to be weighed should be placed on the left-hand balance pan and the weights upon the right-hand pan. Every substance which could attack the metal of the balance pan should be weighed upon a watch-glass, and all objects must be dry and cold. A warm body gives rise to air currents which vitiate the accuracy of the weighing. The weights should be applied in the order in which they occur in the weight-box (not at haphazard), beginning with the largest weight which is apparently required. After a weight has been placed upon the pan the beam should be lowered upon its knife-edges, and, if necessary, the pan-arrests depressed. The movement of the pointer will then indicate whether the weight applied is too great or too small. When the weight has been ascertained, by the successive addition of small weights, to the nearest 5 or 10 milligrams, the weighing is completed by the use of the rider. The correct weight is that which causes the pointer to swing an equal number of divisions to the right and left of the zero-point, when the pointer traverses not less than five divisions on either side. |
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