An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 24 of 272 (08%)
page 24 of 272 (08%)
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deranged or if any substance is spilled upon the pans or in the
balance case, the damage should be reported at once. In many instances serious harm can be averted by prompt action when delay might ruin the balance. Samples for analysis are commonly weighed in small tubes with cork stoppers. Since the stoppers are likely to change in weight from the varying amounts of moisture absorbed from the atmosphere, it is necessary to confirm the recorded weight of a tube which has been unused for some time before weighing out a new portion of substance from it. WEIGHTS The sets of weights commonly used in analytical chemistry range from 20 grams to 5 milligrams. The weights from 20 grams to 1 gram are usually of brass, lacquered or gold plated. The fractional weights are of German silver, gold, platinum or aluminium. The rider is of platinum or aluminium wire. The sets of weights purchased from reputable dealers are usually sufficiently accurate for analytical work. It is not necessary that such a set should be strictly exact in comparison with the absolute standard of weight, provided they are relatively correct among themselves, and provided the same set of weights is used in all weighings made during a given analysis. The analyst should assure himself that the weights in a set previously unfamiliar to him are relatively correct by a few simple tests. For example, he should make sure that in his set two weights of the same denomination (i.e., two |
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