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An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 26 of 272 (09%)
A burette is made from a glass tube which is as uniformly cylindrical
as possible, and of such a bore that the divisions which are etched
upon its surface shall correspond closely to actual contents.

The tube is contracted at one extremity, and terminates in either a
glass stopcock and delivery-tube, or in such a manner that a piece of
rubber tubing may be firmly attached, connecting a delivery-tube of
glass. The rubber tubing is closed by means of a glass bead. Burettes
of the latter type will be referred to as "plain burettes."

The graduations are usually numbered in cubic centimeters, and the
latter are subdivided into tenths.

One burette of each type is desirable for the analytical procedures
which follow.


PREPARATION OF A BURETTE FOR USE

The inner surface of a burette must be thoroughly cleaned in order
that the liquid as drawn out may drain away completely, without
leaving drops upon the sides. This is best accomplished by treating
the inside of the burette with a warm solution of chromic acid in
concentrated sulphuric acid, applied as follows: If the burette is of
the "plain" type, first remove the rubber tip and force the lower
end of the burette into a medium-sized cork stopper. Nearly fill the
burette with the chromic acid solution, close the upper end with a
cork stopper and tip the burette backward and forward in such a way
as to bring the solution into contact with the entire inner surface.
Remove the stopper and pour the solution into a stock bottle to be
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