An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 35 of 272 (12%)
page 35 of 272 (12%)
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vessel or by gently blowing out the last drops. Either practice, when
adopted, must be uniformly adhered to.] FLASKS !Graduated or measuring flasks! are similar to the ordinary flat-bottomed flasks, but are provided with long, narrow necks in order that slight variations in the position of the meniscus with respect to the graduation shall represent a minimum volume of liquid. The flasks must be of such a capacity that, when filled with the specified volume, the liquid rises well into the neck. GRADUATION OF FLASKS It is a general custom to purchase the flasks ungraduated and to graduate them for use under standard conditions selected for the laboratory in question. They may be graduated for "contents" or "delivery." When graduated for "contents" they contain a specified volume when filled to the graduation at a specified temperature, and require to be washed out in order to remove all of the solution from the flask. Flasks graduated for "delivery" will deliver the specified volume of a liquid without rinsing. A flask may, of course, be graduated for both contents and delivery by placing two graduation marks upon it. PROCEDURE.--To calibrate a flask for !contents!, proceed as follows: Clean the flask, using a chromic acid solution, and dry it carefully outside and inside. Tare it accurately; pour water into the flask |
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