Scientific American Supplement, No. 483, April 4, 1885 by Various
page 46 of 111 (41%)
page 46 of 111 (41%)
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In 8 ounces of absolute alcohol dissolve 5 drachms of anhydrous bromide of cadmium. The solution will be milky. Let it stand at least twenty-four hours, or until perfectly clear; it will deposit a white powder. Decant carefully into an 8-ounce bottle, and add to it a drachm of strong hydrochloric acid. Label this "bromide solution;" and it is well to add on the label the constituents, which will be found to be nearly: Alcohol. 1 ounce. Bromide of cadmium. 32 grains. Hydrochloric acid. 8 drops. This solution will keep for ever, and will be sufficient to last two or three years, and with this at hand you will be able in two days to prepare a batch of plates at any time. In doing so, you should proceed thus: Make up your mind how many plates you mean to make, and take of the above accordingly. For two dozen ½-plates or four dozen 3¼ by 3¼, dissolve by heat over, but not too near, a spirit lamp, and by yellow light, 40 grains of nitrate of silver in 1 ounce of alcohol 0.820. While this is dissolving in a little Florence flask on a retort stand at a safe distance from the lamp--which it will do in about 5 minutes--take of the bromized solution ½ an ounce, of absolute ether 1 ounce, of gun-cotton grains; put these in a clean bottle, shake once or twice, and the gun-cotton, if good, will entirely dissolve. As soon as the silver is all dissolved, and while quite hot, pour out the above bromized collodion into a clean 4-ounce measure, having ready in it a clean slip of glass. Pour into it the hot solution of silver in a continuous stream, stirring rapidly all the while with a glass rod. The result will be a perfectly smooth emulsion without lumps or deposit, containing, with sufficient exactitude for all practical purposes, 8 grains of bromide, 16 grains of |
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