A System of Instruction in the Practical Use of the Blowpipe - Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations by Anonymous
page 22 of 359 (06%)
page 22 of 359 (06%)
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dark part of the flame, become reduced and, _in statu nascendi_,
evaporated; but by passing through the external part of the flame, they become oxidized again, and impart a color to the flame. The spirit flame is the most efficient one for the examination of substances the nature of which we wish to ascertain through color imparted to the flame, as that of the spirit-lamp being colorless, is, consequently, most easily and thoroughly recognized by the slightest tinge imparted to it. It is necessary that in operating with such minute quantities of substances as are used in blowpipe analysis, that they should have some appropriate support. In order that no false results may ensue, it is necessary that the supports should be of such a nature that they will not form a chemical combination with the substance while it is exposed to fusion or ignition. Appropriate supports for the different blowpipe experiments are charcoal, platinum instruments, and glass tubes. (_a._) _Charcoal._--The value of charcoal as a support may be stated as follows: 1. The charcoal is infusible, and being a poor conductor of heat, a substance can be exposed to a higher degree of heat upon it than upon any other substance. 2. It is very porous, and therefore allows easily fusible substances (such as alkalies and fluxes) to pass into it, while other substances less fusible, such as metals, to remain unabsorbed. |
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