A System of Instruction in the Practical Use of the Blowpipe - Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations by Anonymous
page 74 of 359 (20%)
page 74 of 359 (20%)
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produce a yellowish flame for a while, until the carbonic acid is
driven off, when the red color of the lime may be discerned. If the borate or phosphate of lime be used, the green color of the acids predominates over the red of the lime. Baryta also destroys the red color of the lime, by mixing its green color with it. There is but one silicate of lime which colors the flame red, it is the variety termed tabular spar. 5. EXAMINATIONS IN THE BORAX BEAD. In order to examine a substance in borax, the loop of the platinum wire should, after being thoroughly cleaned, and heated to redness, be quickly dipped into the powdered borax, and then quickly transferred to the flame of oxidation, and there fused. If the bead is not large enough to fill the loop of the wire, it must be subjected again to the same process. By examining the bead, both when hot and cold, by holding it up against the light, it can be soon ascertained whether it is free from dirt by the transparency, or the want of it, of the bead. In order to make the examination of a substance, the bead should be melted and pressed against it, when enough will adhere to answer the purpose. This powder should then be fused in the oxidation flame until it mixes with, and is thoroughly dissolved by the borax bead. The principal objects to be determined now are: the color of the borax bead, both when heated and when cooled; also the rapidity with which the substance dissolves in the bead, and if any gas is eliminated. |
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