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A System of Instruction in the Practical Use of the Blowpipe - Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations by Anonymous
page 8 of 359 (02%)
The principal operations with the Blowpipe may be explained briefly as
follows:


(_a._) By _Ignition_ is meant the exposure of a substance to such a
degree of heat, that it glows or emits light, or becomes red-hot. Its
greatest value is in the separation of a volatile substance from one
less volatile, or one which is entirely fixed at the temperature of
the flame. In this case we only take cognizance of the latter or fixed
substance, although in many instances we make use of ignition for the
purpose of changing the conditions of a substance, for example, the
sesquioxide of chromium (Cr^{2}O^{3}) in its insoluble modification;
and as a preliminary examination for the purpose of ascertaining
whether the subject of inquiry be a combination of an organic or
inorganic nature.

The apparatus used for this purpose are crucibles of platinum or
silver, platinum foil, a platinum spoon, platinum wire or tongs,
charcoal, glass tubes, and iron spoons.


(_b._) _Sublimation_ is that process by which we convert a solid
substance into vapor by means of a strong heat. These vapors are
condensed by refrigeration into the solid form. It may be termed a
distillation of a solid substance. Sublimation is of great consequence
in the detection of many substances; for instance, arsenic, antimony,
mercury, etc.

The apparatus used for the purposes of sublimation consist of glass
tubes closed at one end.
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