Scientific American Supplement, No. 613, October 1, 1887 by Various
page 45 of 148 (30%)
page 45 of 148 (30%)
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paraffin oil, being the oil obtained direct from the destructive
distillation of shale in retorts; (2) green paraffin oil, which is yielded by distilling or re-running the crude paraffin oil, and removing the lighter or more inflammable portion by fractional distillation; and (3) blue paraffin oil, which is obtained by rectifying the twice run oil with sulphuric acid and soda, and distilling off the paraffin spirit, burning oil, and intermediate oil, and freezing out the solid paraffin as paraffin scale. The best practical trials were obtained in Pintsch's apparatus and in Keith's apparatus. After describing both of these, Dr. Macadam went on to give in great detail the results obtained in splitting up blue paraffin oil into gas in each apparatus. He then said that these experimental results demonstrated that Pintsch's apparatus yielded from the gallon of oil in one case 90.70 cubic feet of gas of 62.50 candle power, and in the second case 103.36 cubic feet of 59.15 candle gas, or an average of 97.03 cubic feet of 60.82 candle power gas. In both cases, the firing of the retorts was moderate, though in the second trial greater care was taken to secure uniformity of heat, and the oil was run in more slowly, so that there was more thorough splitting up of the oil into permanent gas. The gas obtained in the two trials was of high quality, owing to its containing a large percentage of heavy hydrocarbons, of which there were, respectively, 39.25 and 37.15 per cent., or an average of 38.2 per cent., while the sulphureted hydrogen was nothing, and the carbonic acid a mere trace. Besides testing the gas on the occasion of the actual trials, he had also examined samples of the gas which he had taken from various cylinders in which the gas had been stored for several months under a |
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