Hemp Hurds as Paper-Making Material - United States Department of Agriculture, Bulletin No. 404 by Lyster Hoxie Dewey;Jason L. Merrill
page 20 of 40 (50%)
page 20 of 40 (50%)
![]() | ![]() |
|
were charged into the rotary with the addition of a caustic-soda
solution, such as is regularly employed in pulp mills and which tested an average of 109.5 grams of caustic soda per liter, or 0.916 pound per gallon, and averaged 85 per cent causticity. Sufficient caustic solution was added to furnish 25 or 30 per cent of actual caustic soda, calculated on the bone-dry weight of hurds in the charge. After closing the rotary head, it was started rotating at the rate of one-half revolution per minute, and in about five minutes steam at 120 pounds per square inch was admitted at such a rate that the charge was heated in one hour to 170° C., which is the theoretical equivalent of 100 pounds of steam pressure per square inch. It was found, however, that when the temperature reached 170° C. the pressure was usually 115 or 120 pounds instead of 100 pounds, due to air and gases inclosed in the rotary. At this point the rotary was stopped and steam and air relieved until the pressure dropped to 100 pounds, or a solid steam pressure. The temperature was maintained at this point for the number of hours required to reduce the hurds, which was found to be about five, after which the rotary was stopped and steam relieved until the pressure was reduced to zero, when the head was removed and the stock was emptied into a tank underneath, measuring 5-1/2 by 6 by 2 feet deep, where it was drained and washed. Samples of waste soda solution or "black liquor," which were taken from some of the "cooks" for analysis, were drawn while the stock was being thus emptied into the drainer. _Determination of yield._--For determining the yield of cellulose fiber the stock in the drain tank was washed with water until free from waste soda solution, when, by means of a vacuum pump communicating with the space between the bottom and the false perforated bottom, the water was sucked from the stock, leaving the fiber with a very uniform moisture content throughout its entire mass and in a condition suitable for |
|