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Transactions of the American Society of Civil Engineers, vol. LXX, Dec. 1910 - Federal Investigations of Mine Accidents, Structural - Materials and Fuels. Paper No. 1171 by Herbert M. Wilson
page 15 of 187 (08%)
this test if all ten shots fail to ignite the mixture.

“TEST 2.--Ten shots with charge as previously noted, in its original
wrapper, shall be fired, each with 1 pound of clay tamping at a
gallery temperature of 77° F., into a mixture of gas and air
containing 4 per cent. of methane and ethane and 20 pounds of
bituminous coal dust, 18 pounds of which is to be placed on shelves
laterally arranged along the first 20 feet of the gallery, and 2
pounds to be placed near the inlet of the mixing system in such a
manner that all or part of it will be suspended in the first division
of the gallery. An explosive will pass this test if all ten shots fail
to ignite the mixture.

“TEST 3.--Ten shots with charge as previously noted, in its original
wrapper, shall be fired, each with 1 pound of clay tamping at a
gallery temperature of 77° F., into 40 pounds of bituminous coal dust,
20 pounds of which is to be distributed uniformly on a horse placed in
front of the cannon and 20 pounds placed on side shelves in sections
4, 5, and 6. An explosive will pass this test if all ten shots fail to
ignite the mixture.

“TEST 4.--A limit charge will be determined within 25 grams by firing
charges in their original wrappers, untamped, at a gallery temperature
of 77° F., into a mixture of gas and air containing 4 per cent. of
methane and ethane and 20 pounds of bituminous coal dust, to be
arranged in the same manner as in test 2. This limit charge is to be
repeated five times under the same conditions before being
established.

“NOTE.--At least 2 pounds of clay tamping will be used with
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