A Textbook of Assaying: For the Use of Those Connected with Mines. by John Jacob Beringer;Cornelius Beringer
page 38 of 691 (05%)
page 38 of 691 (05%)
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be of the Cornish type, short and open, not long and narrow. For
calcinations, _roasting dishes_ are useful: these are broad and shallow, not unlike saucers, but unglazed. In those cases in which the products of the roasting are liquid at the temperature used, a _scorifier_ (fig. 38) is suitable if it is desired to keep the liquid; but if the liquid is best drained off as quickly as it is formed, a _cupel_ (fig. 5) should be used. [Illustration: FIG. 5.] A scorifier is essentially a roasting dish sufficiently thick to resist, for a time, the corrosive action of the fused metallic oxides it is to contain. The essential property of a cupel is, that it is sufficiently porous to allow the fused oxide to drain into it as fast as it is formed. It should be large enough to absorb the whole of the liquid; and of course must be made of a material upon which the liquid has no corrosive action. Cupels do not bear transport well; hence the assayer generally has to make them, or to supervise their making. A quantity of bone ash is carefully mixed with water so that no lumps are formed, and the mixture is then worked up by rubbing between the hands. The bone ash is sufficiently wet when its cohesion is such that it can be pressed into a lump, and yet be easily crumbled into powder. Cupel moulds should be purchased. They are generally made of turned iron or brass. They consist of three parts (1) a hollow cylinder; (2) a disc of metal; and (3) a piston for compressing the bone ash and shaping the top of the cupel. The disc forms a false bottom for the cylinder. This is put in its place, and the cylinder filled (or nearly so) with the moistened bone ash. The bone ash is then pressed into shape with the piston, and the cupel finished with the help of three or four smart blows from a mallet. Before removing the piston, turn it half-way round upon its axis |
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