A Textbook of Assaying: For the Use of Those Connected with Mines. by John Jacob Beringer;Cornelius Beringer
page 40 of 691 (05%)
page 40 of 691 (05%)
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[Illustration: FIG. 9.]
[Illustration: FIG. 10.] The coke used should be of good quality; the formation of a fused ash (clinker), in any quantity, causes ceaseless trouble, and requires frequent removal. The coke should be broken into lumps of a uniform size (about 2 in. across) before being brought into the office. The furnace should be well packed by stirring, raising the coke and not ramming it, and it should be uniformly heated, not hot below and cold above. In lighting a furnace, a start is made with wood and charcoal, this readily ignites and sets fire to the coke, which of itself does not kindle easily. In commencing work, add (if necessary) fresh coke, and mix well; make hollows, and into these put old crucibles; pack around with coke, so that the surface shall be concave, sloping upwards from the mouths of the crucibles to the sides of the furnace; close the furnace, and, when uniformly heated, substitute for the empty crucibles those which contain the assays. It is rarely advisable to have a very hot fire at first, because with a gradual heat the gases and steam quietly escape through the unfused mass, while with too strong a heat these might make some of the matter in the crucible overflow. Moreover, if the heat should be too strong at first, the flux might melt and run to the bottom of the crucible, leaving the quartz, &c., as a pasty mass above; with a gentler heat combination is completed, and the subsequent fiercer heat simply melts the fusible compound into homogeneous slag. The fused material may be left in the crucible and separated from it by breaking when cold. It is generally more convenient to pour it into |
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