A Textbook of Assaying: For the Use of Those Connected with Mines. by John Jacob Beringer;Cornelius Beringer
page 44 of 691 (06%)
page 44 of 691 (06%)
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over for assaying along with the next batch. If one filters slowly or is
in any way less forward than the rest, it may lessen the accuracy of the other assays, owing to oxidation, &c., it should, therefore, be put on one side. The assays are dealt with in batches of ten or twenty, so that a large quantity of work can be quickly finished. [Illustration: FIG. 11.] When the assays are finished, it is the duty of the assistant to clean the apparatus (with reagents, if necessary), and to put the vessels in the place set apart for them. Flasks are best kept inverted on a rack, so that they may be dry and clean by the next morning. Berlin crucibles must be cleaned and ignited. The amount of apparatus employed should be as little as is feasible. The assay should be carried out as much as possible in the same flask. The bench must be clean, and altogether free from apparatus not in actual use. Crucibles and dishes in which weighings are made should be marked with numbers or letters; and their weights recorded, together with the date of weighing, in a small ledger, which is kept in the drawer of the balance. By this means a record of the "wear" of each piece of apparatus is obtained, and, what is more important, much weighing is saved, and increased confidence is gained. The weight of each piece of apparatus need not be taken daily. It will be seen from the record in the book and a knowledge of the use it has been put to how often a checking of the weight is necessary. The entries are made in black lead as follows:-- Dish, A. Feb. 3 9.4210 grams. 5 9.4225 6 9.4230 |
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