A Textbook of Assaying: For the Use of Those Connected with Mines. by John Jacob Beringer;Cornelius Beringer
page 75 of 691 (10%)
page 75 of 691 (10%)
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a 100 c.c. flask to a beaker, it will be necessary to complete the
transfer by rinsing out the flask and adding the washings; otherwise there will be a sensible loss. Graduated cylinders (fig. 28) are convenient for preparing standard solutions. [Illustration: FIG. 27.] [Illustration: FIG. 28.] [Illustration: FIG. 29.] ~Pipettes~ and burettes are graduated to _deliver_ the quantities specified. The principle of the pipette, and the advantages and disadvantages of its various forms, may be understood by considering the first form shown in fig. 29. It is essentially a bulbed tube drawn out to a jet at its lower end, and having on each side of the bulb a mark so placed that when the surface of the liquid falls from the upper to the lower mark the instrument shall deliver exactly 100 c.c. The bore of the jet should be of such a size as will allow the level of the liquid to fall at the rate of about one foot in two minutes. If it runs more quickly than this, an appreciable error arises from the varying amount of liquid remaining, and damping the sides of the bulb. The flow of liquid from a pipette must not be hastened by blowing into it. The lower tube or nose of the pipette should be long enough to reach into the bottle or flask containing the liquid about to be measured. The pipette is filled by sucking at the open end with the mouth; this method of filling renders the use of the instrument dangerous for such liquids as strong acids, ammonia, and such poisonous solutions as that of potassic cyanide. One attempt with a fairly strong solution of ammonia will teach the beginner a very useful lesson. As soon as the liquid rises above the |
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