An Introduction to Chemical Science by Rufus Phillips Williams
page 37 of 262 (14%)
page 37 of 262 (14%)
![]() | ![]() |
|
hand. Only a mere opening is made in this way, which must be
enlarged by the other end of the file. A second or third file of larger size may be employed, according to the size of the hole to be made, which must be a little smaller than the tube it is to receive, and perfectly round. CHAPTER VI. OXYGEN. 22. To Obtain Oxygen. Experiment 13.--Take 5 g. of crystals of potassium chlorate (KClO3) and, without pulverizing, mix with the same weight of pure powdered manganese dioxide (MnO2). Put the mixture into a t.t., and insert a d.t.--delivery-tube--having the cork fit tightly. Hang it on a r.s.--ring-stand,-- as in Figure 7, having the other end of the d.t. (Fig 7.) under the shelf, in a pneumatic trough, filled with water just above the shelf. Fill three or more receivers--wide-mouthed bottles--with water, cover the mouth of each with a glass plate, invert it with its mouth under water, and put it on the shelf of the trough, removing the plate. No air should be in the bottles. Have the end of the d.t. so that the gas will rise through the orifice. Hold a lighted lamp in the hand, and bring the flame against the mixture in the t.t. Keep |
|