Scientific American Supplement, No. 288, July 9, 1881 by Various
page 19 of 160 (11%)
page 19 of 160 (11%)
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of 11 parts of oxygen mixture--a suitable quantity for all coals
exported--would enable operators to obtain similar figures, and make the test uniform in different hands. The following is a brief outline of the method of procedure recommended: Sample the coal until an average portion passes through a sieve having 64 meshes to the square inch. Take about 300 grains (20 grammes) of this and run through a brass wire gauze having 4,600 meshes to the square inch, taking care that the whole sample selected is thus treated. One part of nitrate of potash and 3 parts of chlorate of potash (dry) are separately ground in a mortar, and repeatedly sifted through another wire gauze sieve, having 1,000 meshes to the square inch, in order that the oxygen mixture shall _not_ be ground to an impalpable powder, as this is very undesirable. It absorbs moisture rapidly, and interferes with the regularity of the combustion when very fine. 330 grains of the powder are weighed out (after drying), and intimately incorporated with 30 grains of coal--better with a spatula than by rubbing in a mortar--and then introduced into a copper cylinder (31/2 inches long by 3/4 inch wide, made from a copper tube), and pressed down in small portions by a test-tube with such firmness as is required by the nature of the coal, not tapped on the bottom, since the rougher portions of the oxygen mixture rise to the surface. As the temperature of a room is almost invariably much higher than the water supply, a little hot water is added to that placed in the glass cylinder, until the difference of temperature between the water and the room is about the mark indicated in the following table: Room at The water should be 80 deg. F. 70 deg. F. |
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