Scientific American Supplement, No. 384, May 12, 1883 by Various
page 76 of 136 (55%)
page 76 of 136 (55%)
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0.2 grain per ounce | no increase after six hours. | 2.0 " " | about one-half an hour. | 20.0 " " | seven minutes. | --------------------------+------------------------------+ I must here leave the _rationale_ of the process for the present, and proceed with the next operation. Our emulsion being cold, I add to it, for every 6 ounces of mixed emulsion, 1 ounce of a saturated cold solution of potassium bichromate; then, gently swirling the mixture round, a few drops of a dilute (1 to 8) solution of hydrochloric acid, and place it on one side for a minute or two. When hydrochloric acid is added to bichromate of potash, chromic acid is liberated. Now, chromic acid has the property of precipitating gelatine, so that what I hope to have done is to have precipitated the gelatine in this emulsion, and which will carry down the silver bromide as well. You see here I can pour off the supernatant liquid clear, leaving our silver and gelatine as a clot at the bottom of the vessel. Another action of chromic acid is, that it destroys the action of light on silver bromide, so that up to this point operations can be carried on in broad daylight. The precipitated emulsion is now taken into the dark room and washed until the wash water shows no trace of color; if there be a large quantity, this is best done on a fine muslin filter; if a small quantity, by decantation. |
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