Scientific American Supplement, No. 447, July 26, 1884 by Various
page 61 of 141 (43%)
page 61 of 141 (43%)
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wool, the greasy matter is dissolved, and along with the solvent enters
a reservoir. The machine is now set in motion, and the bulk of the solvent is drawn off. Cold water is then admitted, and the machine being again caused to rotate, the whole of the bisulphide is expelled. It is a curious fact that, although wool soaks remarkably easily with carbon disulphide, and at once becomes wet, cold water expels and replaces almost all that liquid. This operation takes about twenty minutes, and at one operation about 11/2 cwt. of raw wool may be treated. The wool is then washed in suitable washing machines of the ordinary type, but with cold water, no soap or alkali being employed. The bisulphide of carbon, mixed with water, flows into a reservoir, provided with diaphragms to prevent splashing, and consequent loss by evaporation. From its gravity it sinks, forming a layer below the water; it is then separated and recovered by distillation, and may be used in subsequent operations. The point in which this process differs from the old and unsuccessful ones formerly tried, is in the expulsion of the carbon disulphide. It was imagined that it was necessary to expel it by means of heat or steam. Now, when wool moist with bisulphide is heated, it invariably turns yellow. No heat must, therefore, be employed. As already remarked, the solvent is expelled with cold water. The residue, after distillation of the carbon disulphide, is a grayish colored, very viscous oily matter, still retaining a little bisulphide, as may be perceived from the smell. It has not the composition of ordinary _suint_, inasmuch as it contains no carbonate of potash, and indeed little mineral matter of any kind. A sample which I analyzed lost in drying 36.2 per cent., the loss consisting of water and carbon disulphide. It gave a residue on ignition amounting only to 1.6 per cent. of the original fatty matter, or 2.5 per cent. of the dried fat. |
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