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An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 28 of 272 (10%)

If air bubbles escape during subsequent calibration or titration, an
error is introduced which vitiates the results.]


READING OF A BURETTE

All liquids when placed in a burette form what is called a meniscus at
their upper surfaces. In the case of liquids such as water or
aqueous solutions this meniscus is concave, and when the liquids are
transparent accurate readings are best obtained by observing the
position on the graduated scales of the lowest point of the meniscus.
This can best be done as follows: Wrap around the burette a piece of
colored paper, the straight, smooth edges of which are held evenly
together with the colored side next to the burette (Note 1). Hold the
paper about two small divisions below the meniscus and raise or lower
the level of the eyes until the edge of the paper at the back of the
burette is just hidden from the eye by that in front (Note 2). Note
the position of the lowest point of the curve of the meniscus,
estimating the tenths of the small divisions, thus reading its
position to hundredths of a cubic centimeter.

[Note 1: The ends of the colored paper used as an aid to accurate
readings may be fastened together by means of a gummed label. The
paper may then remain on the burette and be ready for immediate use by
sliding it up or down, as required.]

[Note 2: To obtain an accurate reading the eye must be very nearly on
a level with the meniscus. This is secured by the use of the paper
as described. The student should observe by trial how a reading is
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