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An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 29 of 272 (10%)
affected when the meniscus is viewed from above or below.

The eye soon becomes accustomed to estimating the tenths of the
divisions. If the paper is held as directed, two divisions below the
meniscus, one whole division is visible to correct the judgment. It is
not well to attempt to bring the meniscus exactly to a division mark
on the burette. Such readings are usually less accurate than those in
which the tenths of a division are estimated.]


CALIBRATION OF GLASS MEASURING DEVICES

If accuracy of results is to be attained, the correctness of all
measuring instruments must be tested. None of the apparatus offered
for sale can be implicitly relied upon except those more expensive
instruments which are accompanied by a certificate from the !National
Bureau of Standards! at Washington, or other equally authentic source.

The bore of burettes is subject to accidental variations, and since
the graduations are applied by machine without regard to such
variations of bore, local errors result.

The process of testing these instruments is called !calibration!.
It is usually accomplished by comparing the actual weight of water
contained in the instrument with its apparent volume.

There is, unfortunately, no uniform standard of volume which has been
adopted for general use in all laboratories. It has been variously
proposed to consider the volume of 1000 grams of water at 4°, 15.5°,
16°, 17.5°, and even 20°C., as a liter for practical purposes, and to
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