An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 33 of 272 (12%)
page 33 of 272 (12%)
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The student should clearly understand that !all other weighings!, except those for calibration, should be made accurately to 0.0001 gram, unless special directions are given to the contrary. Corrections for temperature variations of less than 4°C. are negligible, as they amount to less than 0.01 gram for each 10 grams of water withdrawn.] [Note 3: Should the error discovered in any interval of 10 cc. on the burette exceed 0.10 cc., it is advisable to weigh small portions (even 1 cc.) to locate the position of the variation of bore in the tube rather than to distribute the correction uniformly over the corresponding 10 cc. The latter is the usual course for small corrections, and it is convenient to calculate the correction corresponding to each cubic centimeter and to record it in the form of a table or calibration card, or to plot a curve representing the values. Burettes may also be calibrated by drawing off the liquid in successive portions through a 5 cc. pipette which has been accurately calibrated, as a substitute for weighing. If many burettes are to be tested, this is a more rapid method.] PIPETTES A !pipette! may consist of a narrow tube, in the middle of which is blown a bulb of a capacity a little less than that which it is desired to measure by the pipette; or it may be a miniature burette, without |
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