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An Introductory Course of Quantitative Chemical Analysis - With Explanatory Notes by Henry P. Talbot
page 33 of 272 (12%)

The student should clearly understand that !all other weighings!,
except those for calibration, should be made accurately to 0.0001
gram, unless special directions are given to the contrary.

Corrections for temperature variations of less than 4°C. are
negligible, as they amount to less than 0.01 gram for each 10 grams of
water withdrawn.]

[Note 3: Should the error discovered in any interval of 10 cc. on the
burette exceed 0.10 cc., it is advisable to weigh small portions (even
1 cc.) to locate the position of the variation of bore in the
tube rather than to distribute the correction uniformly over the
corresponding 10 cc. The latter is the usual course for small
corrections, and it is convenient to calculate the correction
corresponding to each cubic centimeter and to record it in the form
of a table or calibration card, or to plot a curve representing the
values.

Burettes may also be calibrated by drawing off the liquid in
successive portions through a 5 cc. pipette which has been accurately
calibrated, as a substitute for weighing. If many burettes are to be
tested, this is a more rapid method.]


PIPETTES

A !pipette! may consist of a narrow tube, in the middle of which is
blown a bulb of a capacity a little less than that which it is desired
to measure by the pipette; or it may be a miniature burette, without
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