Scientific American Supplement, No. 832, December 12, 1891 by Various
page 115 of 147 (78%)
page 115 of 147 (78%)
![]() | ![]() |
|
red, between wave lengths 744 and 623. Their positions and relative
intensities are as follows: [lambda] = 744 very feeble. | [lambda] = 685.5 feeble 740 " | 683.5 " 734 " | 677 strong 714 feeble. | 640.5 " 704 " | 634 " 691 " | 623 " 687.5 " | At a temperature of -95° at ordinary atmospheric pressure, fluorine remains gaseous, no sign of liquefaction having been observed. METHODS OF EXPERIMENTING WITH FLUORINE. When it is desired to determine the action of fluorine upon a solid substance, the following method of procedure is adopted. A preliminary experiment is first made, in order to obtain some idea as to the degree of energy of the reaction, by bringing a little of the solid, placed upon the lid of a platinum crucible held in a pair of tongs, near the mouth of the delivery tube of the preparation apparatus. If a gaseous or liquid product results, and it is desirable to collect it for examination, small fragments of the solid are placed in a platinum tube connected to the delivery tube by flexible platinum tubing or by a screw joint, and the resulting gas may be collected over water or mercury, or the liquid condensed in a cooled cylinder of platinum. In this manner the action of fluorine upon sulphur and iodine has been studied. If the solid, phosphorus for instance, attacks platinum, or |
|