A System of Instruction in the Practical Use of the Blowpipe - Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations by Anonymous
page 18 of 359 (05%)
page 18 of 359 (05%)
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or to the oxide of molybdenum. The flame of oxidation will again
convert this oxide into the acid, and this conversion is a good test of the progress of the student in the use of the blowpipe. In cases where we have to separate a more oxidizable substance from a less one, we use with success the blue cone, particularly if we wish to determine whether a substance has the quality, when submitted to heat in the blue cone, of coloring the external flame. A good _reduction_ flame can be obtained by the use of a small orifice at the point of the blowpipe. In order to produce such a flame, hold the point of the blowpipe higher above the wick, while the nozzle must not enter the flame so far as in the production of the oxidation flame. The point of the blowpipe should only touch the flame, while the current of air blown into it must be stronger than into the oxidation flame. If we project a stream, in the manner mentioned, into the flame, from the smaller side of the wick to the middle, we shall perceive the flame changed to a long, narrow, luminous cone, _a b_, Fig. 4, the end _a_ of which is enveloped by the same dimly visible blueish colored portion of the flame _a, c_, which we perceive in the original flame, with its point at _c_. The portion close above the wick, presenting the dull appearance, is occasioned by the rising gases which have not supplied to them enough oxygen to consume them entirely. The hydrogen is consumed, while the carbon is separated in a state of bright ignition, and forms the internal flame. [Illustration: Fig. 4] Directly above the wick, the combustion of the gases is least complete, and forms there likewise, as is the case in the free flame, a dark blue nucleus _d_. |
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