A System of Instruction in the Practical Use of the Blowpipe - Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations by Anonymous
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page 20 of 359 (05%)
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of manganese with borax, upon a platinum wire, in the oxidation flame,
when a violet-red glass will be obtained; or if too much of the oxide be used, a glass of a dark color and opaque will be obtained. By submitting this glass to the reduction flame, it will become colorless in correspondence to the perfection with which the flame is produced. Or a piece of tin may be fused upon charcoal, and kept in that state for a considerable time, while it presents the appearance of a bright metal on the surface. This will require dexterity in the operator; for, if the oxidation flame should chance to touch the bright metal only for a moment, it is coated with an infusible oxide. COMBUSTION.--Any flame of sufficient size can be used for blowpipe operations. It may be either the flame of a candle of tallow or wax, or the flame of a lamp. The flame of a wax candle, or of an oil lamp is most generally used. Sometimes a lamp is used filled with a solution of spirits of turpentine in strong alcohol. If a candle is used, it is well to cut the wick off short, and to bend the wick a little toward the substance experimented upon. But candles are not the best for blowpipe operations, as the radiant heat, reflecting from the substance upon the wax or tallow, will cause it to melt and run down the side of the candle; while again, candles do not give heat enough. The lamp is much the most desirable. The subjoined figure, from Berzelius, is perhaps the best form of lamp. It is made of japanned tin-plate, about four inches in length, and has the form and arrangement represented in Fig. 5. K is the lamp, fastened on the stand, S, by a screw, C, and is movable upwards or downwards, as represented in the figure. The posterior end of the lamp may be about one inch square, and at its anterior end, E, about three-quarters of an inch square. The under side of this box may be round, as seen in |
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