A System of Instruction in the Practical Use of the Blowpipe - Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations by Anonymous
page 38 of 359 (10%)
page 38 of 359 (10%)
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unsteady flame produced by too strong a blast. The reason is an
incomplete fusion, while from the basic borate compound a part of the base is separated. As the boracic acid is capable of dissolving more in the heat, a bead will be clear while hot, enamelled when cold, as a part in the latter instance will become separated. (2.) Whether the substance dissolves easily or not, and whether it intumesces from arising gases. (3.) Whether the bead, when exposed to the oxidation flame, exhibits any color, and whether the color remains after the bead shall have cooled, or whether the color fades. (4.) Whether the bead exhibits any other reaction in the reduction flame. The bead should not be overcharged with the substance under examination, or it will become colored so deeply as not to present any transparency, or the color light enough to discern its hue. 8. _Microcosmic Salt--Phosphate of Soda and Ammonia_--(NaO, NH^{4}O + PO^{5}).--Dissolve six parts of phosphate of soda (2NaO, HO, PO^{5}), and one part of pure chloride of Ammonium (NH^{4}Cl.), in two parts of boiling water, and allow it to cool. The greatest part of the formed double salt crystallizes, while the mother-liquid contains chloride of sodium, and some of the double salt. The crystals must be dissolved in as little boiling water as possible, and re-crystallized. These crystals must be dried and powdered. |
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