A System of Instruction in the Practical Use of the Blowpipe - Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations by Anonymous
page 43 of 359 (11%)
page 43 of 359 (11%)
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used to detect hydrofluoric acid, which changes its color to yellow.
All the test-papers are to be cut into narrow strips, and preserved in closely stopped vials. The especial employment of the test-papers we shall allude to in another place. B. ESPECIAL REAGENTS. 13. _Fused Boracic Acid_ (BO^{3}).--The commercial article is sufficiently pure for blowpipe analysis. It is employed in some cases to detect phosphoric acid, and also minute traces of copper in lead compounds. 14. _Fluorspar_ (CaFl^{2}).--This substance should be pounded fine and strongly heated. Fluorspar is often mixed with boracic acid, which renders it unfit for analytical purposes. Such an admixture can be detected if it be mixed with bisulphate of potassa, and exposed upon platinum wire to the interior or blue flame. It is soon fused, the boracic acid is reduced and evaporated, and by passing through the external flame it is reoxidized, and colors the flame green. We use fluorspar mixed with bisulphate of potassa as a test for lithia and boracic acid in complicated compounds. 15. _Oxalate of Nickel_ (NiO, [=]O).--It is prepared by dissolving the pure oxide of nickel in diluted hydrochloric acid. Evaporate to dryness, dissolve in water, and precipitate with oxalate of ammonia. |
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