A System of Instruction in the Practical Use of the Blowpipe - Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations by Anonymous
page 42 of 359 (11%)
page 42 of 359 (11%)
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dryness. Moisten the dry residue with hydrochloric acid, and boil in
water. The silica remains insoluble. It should be washed well, dried, and heated, and then reduced to powder. 12. TEST-PAPERS.--(_a._) _Blue, Litmus Paper._--Dissolve one part of litmus in six or eight parts of water, and filter. Divide the filtrate into two parts. In one of the parts neutralize the free alkali by stirring it with a glass rod dipped in diluted sulphuric acid, until the fluid appears slightly red. Then mix the two parts together, and draw slips of unsized paper, free from alkali, such as fine filtering paper. Hang these strips on a line to dry, in the shade and free from floating dust. If the litmus solution is too light, it will not give sufficient characteristic indications, and if too dark it is not sensitive enough. The blue color of the paper should be changed to red, when brought in contact with a solution containing the minutest trace of free acid; but it should be recollected that the neutral salts of the heavy metals produce the same change. (_b._) _Red Litmus Paper._--The preparation of the red litmus paper is similar to the above, the acid being added until a red color is obtained. Reddened litmus paper is a very sensitive reagent for free alkalies, the carbonates of the alkalies, alkaline earths, sulphides of the alkalies and of the alkaline earths, and alkaline salts with weak acids, such as boracic acid. These substances restore the original blue color of the litmus. (_c._) _Logwood Paper._--Take bruised logwood, boil it in water, filter, and proceed as above. Logwood paper is a very delicate test for free alkalies, which impart a violet tint to it. It is sometimes |
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