A System of Instruction in the Practical Use of the Blowpipe - Being A Graduated Course Of Analysis For The Use Of Students And All Those Engaged In The Examination Of Metallic Combinations by Anonymous
page 56 of 359 (15%)
page 56 of 359 (15%)
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sometimes, but quite so with the aid of the magnifying glass.
_Lead_, or its chloride, sublimes like tellurium, and, like that substance, fuses into globules or drops. _Bismuth_, or its sulphide, sublimes into an orange or brownish globules, when it is melted, as directed above, for tellurium. The color of the bismuth and lead oxides are somewhat similar, although that of the latter is paler. If any mineral containing _fluorine_, is fused, first with the microcosmic salt bead, then put into the tube, and the flame of the blowpipe be directed _into_ the tube upon the bead, hydrofluoric acid is disengaged and attacks the inside of the tube. The fluoride of calcium, or fluorspar, may be used for this experiment. During the roasting, a brisk current of air should be allowed to pass through the tube, whereby unoxidized matter may be prevented from volatilization, and the clogging up of the substance under examination be prevented. 3. EXAMINATIONS UPON CHARCOAL. In making examinations upon charcoal, it is quite necessary that the student should make himself familiar with the different and characteristic appearances of the deposits upon the charcoal. In this case I have found the advice given by Dr. Sherer to be the best; that is, to begin with the examination of the pure materials first, until |
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